中文摘要:本文描述了一种简便快速的同时检测硬质及软质小麦面食样品中的17种霉菌毒素的多重霉菌毒素分析方法。
外文摘要:A simple and rapid multi-mycotoxin method for the determination of 17 mycotoxins simultaneously is described in the present survey on durum and soft wheat pasta samples. Mycotoxins included in the study were those mainly reported in cereal samples: ochratoxin-A (OTA), aflatoxin B1 (AFB1), zearalenone (ZON), deoxynivalenol (DON), 3-and 15-acetyl-deoxynivalenol (3-AcDON and 15-AcDON), nivalenol (NIV), neosolaniol (NEO), fusarenon-X, (FUS-X), T-2 toxin (T-2) and HT-2 toxin (HT-2), fumonisin B1 and B2 (FB1 and FB2), and four emerging mycotoxins: three enniatins (ENA, ENA1, and ENB), and beauvericin (BEA). Twenty-nine samples were analyzed to provide an overview on mycotoxin presence: 27 samples of durum wheat pasta, and two samples of baby food. Analytical results concluded that trichothecenes showed the highest incidence, mainly DON, NIV, and HT-2 toxin, followed by ZON and ENB, while NEO, FUS-X, OTA, AFB1, and FUM were not detected in any sample. The highest contents corresponded to ENB and ranged from 91.15μg/kg to 710.90 μg/kg.
外文关键词:baby-food;durum wheat pasta;multi-residual method;HRMS-orbitrap
作者:Tolosa, J;Graziani, G;Gaspari, A;Chianese, D;Ferrer, E;Manes, J;Ritieni, A
作者单位:Univ Valencia
期刊名称:TOXINS
期刊影响因子:3.571
出版年份:2017
出版刊次:2
点击下载:用液相色谱-串联四极杆的Orbitrap质谱分析硬质小麦面食中的多重霉菌毒素