中文摘要：本文采用标准加入法与高效液相色谱法-高分辨四极杆飞行时间质谱法联用识别和检测食品和饲料单样本中492种有毒物质。这些有毒物质包括霉菌毒素、兽药和合成染料。本方法样本筛选耗时40-60分钟，残留测定需要2-3小时，相对标准差小于等于0.15。
外文摘要：The methodology for the identification and determination of 492 different toxicants from a single sample in food and feed by high-resolution quadrupole time-of-flight MS in combination with HPLC has been presented. The sample preparation is easy. The analytes are pesticides of different classes, including mycotoxins, veterinary drugs, and synthetic dyes. A scheme for the identification and determination of toxicants using the standard addition method has been given. The RSDs of the analytical results presented are <= 0.15, with a 40-60 min sample screening time and a 2-3 h for the determination of the detected toxicants.
外文关键词：PERFORMANCE LIQUID-CHROMATOGRAPHY; SOLID-PHASE EXTRACTION; MULTI-RESIDUE METHOD; GAS-CHROMATOGRAPHY; MULTIRESIDUE METHOD; PESTICIDE-RESIDUES; VETERINARY DRUGS; MYCOTOXINS; MATRICES; SAMPLES
作者：Amelin, Vasiliy; Korotkov, Anton; Andoralov, Alexander
作者单位：Fed Ctr Anim Hlth, Vladimir 600901, Russia.
期刊名称：JOURNAL OF AOAC INTERNATIONAL
期刊影响因子：0.918
出版年份：2016
出版刊次：10
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