微分伏安法定量检测t-2毒素

Method for quantitative determination of t-2 toxin by differential voltammetry

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外文摘要:NOVELTY - Invention relates to analytical chemistry and can be used in pharmacokinetic analysis for control of agricultural products of vegetal origin.
 USE - Chemistry.
 ADVANTAGE - Invention provides extending the range of determined concentrations of t-2 toxin and development of rapid evaluation of T-2 toxin for 30-40 minutes and possibility to use electrodes made of nontoxic material.1 cl, 1 dwg, 2 tbl, 2 ex
 DETAILED DESCRIPTION - Invention relates to analytical chemistry and can be used in pharmacokinetic analysis for control of agricultural products of vegetal origin. According to invention, T-2 toxin is transferred from a sample into the solution and voltammetric accumulation of mycotoxin in a stirred solution for 30 s at electrolysis potential (-0.5 plus minus 0.05) v relative a saturated silver chloride electrode on the background of potassium nitrate (KNO3), pH 4.0 divide by 5.0, with subsequent recording of cathode peaks at scanning rate of 30 mV/s. concentration of T-2 toxin were determined by peak height in the range of En=(-1.25 plus minus 0.35) in by standard addition method.
申请号:RU2580412-C1
专利号:RU2580412-C1
公开/公告号:RU103279
申请/专利权人:UNIV TOMSK NAT RES POLYTECH (UYTO-N)
发明/设计人:GAVRILOVA, M A;SLEPCHENKO, G B;DERYABINA, V I
分类号:G01N-027/48
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  1. 编译服务:农产品质量安全
  2. 编译者:虞德容
  3. 编译时间:2016-12-21